WO2007018940A3 - Hydrogen purification for make-up gas in hydroprocessing processes - Google Patents

Hydrogen purification for make-up gas in hydroprocessing processes Download PDF

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Publication number
WO2007018940A3
WO2007018940A3 PCT/US2006/027135 US2006027135W WO2007018940A3 WO 2007018940 A3 WO2007018940 A3 WO 2007018940A3 US 2006027135 W US2006027135 W US 2006027135W WO 2007018940 A3 WO2007018940 A3 WO 2007018940A3
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WO
WIPO (PCT)
Prior art keywords
hydrogen
recycle gas
make
gas compressor
gas
Prior art date
Application number
PCT/US2006/027135
Other languages
French (fr)
Other versions
WO2007018940A2 (en
Inventor
Yuv R Mehra
Ali H Al-Abdulal
Original Assignee
Saudi Arabian Oil Co
Yuv R Mehra
Ali H Al-Abdulal
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Saudi Arabian Oil Co, Yuv R Mehra, Ali H Al-Abdulal filed Critical Saudi Arabian Oil Co
Priority to CN200680034633.8A priority Critical patent/CN101273113B/en
Priority to EP06787087A priority patent/EP1917328A4/en
Priority to CA2620139A priority patent/CA2620139C/en
Priority to KR1020087003928A priority patent/KR101323950B1/en
Publication of WO2007018940A2 publication Critical patent/WO2007018940A2/en
Publication of WO2007018940A3 publication Critical patent/WO2007018940A3/en

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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/24—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions with moving solid particles
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G49/00—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00
    • C10G49/007—Treatment of hydrocarbon oils, in the presence of hydrogen or hydrogen-generating compounds, not provided for in a single one of groups C10G45/02, C10G45/32, C10G45/44, C10G45/58 or C10G47/00 in the presence of hydrogen from a special source or of a special composition or having been purified by a special treatment
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C10G45/04—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used
    • C10G45/06—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used containing nickel or cobalt metal, or compounds thereof
    • C10G45/08—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used containing nickel or cobalt metal, or compounds thereof in combination with chromium, molybdenum, or tungsten metals, or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/1044—Heavy gasoline or naphtha having a boiling range of about 100 - 180 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/1048—Middle distillates
    • C10G2300/1051—Kerosene having a boiling range of about 180 - 230 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1037—Hydrocarbon fractions
    • C10G2300/1048—Middle distillates
    • C10G2300/1055—Diesel having a boiling range of about 230 - 330 °C
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1074—Vacuum distillates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/10—Feedstock materials
    • C10G2300/1096—Aromatics or polyaromatics
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/202—Heteroatoms content, i.e. S, N, O, P
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/20—Characteristics of the feedstock or the products
    • C10G2300/201—Impurities
    • C10G2300/207—Acid gases, e.g. H2S, COS, SO2, HCN
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/42—Hydrogen of special source or of special composition
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
    • C10G2300/40—Characteristics of the process deviating from typical ways of processing
    • C10G2300/44—Solvents

Abstract

The recycle gas stream containing hydrogen that is part of the feedstream to a hydroprocessing reactor is mixed with the low purity make-up hydrogen and the sour flash gases upstream of the recycle gas compressor and compressed by the recycle gas compressor, The compressed gases pass through a methane and higher (C1+) absorber to produce a sweet hydrogen recycle gas stream that is delivered to the hydroprocessing reactor at 96-98 mol% hydrogen. The process can be used to advantage in existing process facilities to increase the hydrogen partial pressure in the feedstream to the hydroprocessor where the existing recycle gas compressor is not designed for compressing the high purity hydrogen.
PCT/US2006/027135 2005-07-20 2006-07-11 Hydrogen purification for make-up gas in hydroprocessing processes WO2007018940A2 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN200680034633.8A CN101273113B (en) 2005-07-20 2006-07-11 Hydrogen purification for make-up gas in hydroprocessing processes
EP06787087A EP1917328A4 (en) 2005-07-20 2006-07-11 Hydrogen purification for make-up gas in hydroprocessing processes
CA2620139A CA2620139C (en) 2005-07-20 2006-07-11 Hydrogen purification for make-up gas in hydroprocessing processes
KR1020087003928A KR101323950B1 (en) 2005-07-20 2006-07-11 Hydrogen purification for make-up gas in hydroprocessing processes

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US11/186,204 US9017547B2 (en) 2005-07-20 2005-07-20 Hydrogen purification for make-up gas in hydroprocessing processes
US11/186,204 2005-07-20

Publications (2)

Publication Number Publication Date
WO2007018940A2 WO2007018940A2 (en) 2007-02-15
WO2007018940A3 true WO2007018940A3 (en) 2007-10-04

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PCT/US2006/027135 WO2007018940A2 (en) 2005-07-20 2006-07-11 Hydrogen purification for make-up gas in hydroprocessing processes

Country Status (6)

Country Link
US (1) US9017547B2 (en)
EP (1) EP1917328A4 (en)
KR (1) KR101323950B1 (en)
CN (1) CN101273113B (en)
CA (1) CA2620139C (en)
WO (1) WO2007018940A2 (en)

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US8999141B2 (en) * 2008-06-30 2015-04-07 Uop Llc Three-phase hydroprocessing without a recycle gas compressor
US8263008B2 (en) * 2008-12-18 2012-09-11 Uop Llc Apparatus for improving flow properties of crude petroleum
US9157037B2 (en) * 2008-12-18 2015-10-13 Uop Llc Process for improving flow properties of crude petroleum
US8518351B2 (en) 2011-03-31 2013-08-27 Uop Llc Apparatus for producing diesel
US8747653B2 (en) 2011-03-31 2014-06-10 Uop Llc Process for hydroprocessing two streams
US8158069B1 (en) 2011-03-31 2012-04-17 Uop Llc Apparatus for mild hydrocracking
US8608940B2 (en) 2011-03-31 2013-12-17 Uop Llc Process for mild hydrocracking
US8753501B2 (en) 2011-10-21 2014-06-17 Uop Llc Process and apparatus for producing diesel
WO2012134838A2 (en) * 2011-03-31 2012-10-04 Uop Llc Process and apparatus for producing diesel
US8158070B1 (en) 2011-03-31 2012-04-17 Uop Llc Apparatus for hydroprocessing two streams
US8696885B2 (en) 2011-03-31 2014-04-15 Uop Llc Process for producing diesel
US8691078B2 (en) 2011-05-17 2014-04-08 Uop Llc Process for hydroprocessing hydrocarbons
US9115318B2 (en) 2011-11-04 2015-08-25 Saudi Arabian Oil Company Hydrocracking process with integral intermediate hydrogen separation and purification
WO2013067323A1 (en) 2011-11-04 2013-05-10 Saudi Arabian Oil Company Hydrotreating and aromatic saturation process with integral intermediate hydrogen separation and purification
US8816144B2 (en) * 2012-10-04 2014-08-26 Gas Technology Institute Direct production of fractionated and upgraded hydrocarbon fuels from biomass
US9084945B2 (en) * 2013-08-19 2015-07-21 Uop Llc Enhanced hydrogen recovery
CN104017604B (en) * 2014-06-25 2016-03-30 清华大学 A kind of device and method of gasifying biomass catalytic reforming biological hydrogen
US9765267B2 (en) 2014-12-17 2017-09-19 Exxonmobil Chemical Patents Inc. Methods and systems for treating a hydrocarbon feed
KR102439330B1 (en) * 2015-11-04 2022-09-02 한국조선해양 주식회사 Hydrate inhibitor treatment system
CN105802686B (en) * 2016-03-08 2019-03-01 安庆凯美特气体有限公司 The method of liquefied gas and pentane is extracted from refinery exhaust
CN110845293A (en) * 2019-11-13 2020-02-28 宁波同润和海科技有限公司 Method for separating methane component in mixed gas by adopting cryogenic absorption principle
CN112239682A (en) * 2020-09-08 2021-01-19 中石化宁波工程有限公司 Gasification device slag water flash evaporation gas comprehensive utilization system and method

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Also Published As

Publication number Publication date
US9017547B2 (en) 2015-04-28
CN101273113B (en) 2015-06-17
US20070017851A1 (en) 2007-01-25
KR101323950B1 (en) 2013-10-31
WO2007018940A2 (en) 2007-02-15
EP1917328A2 (en) 2008-05-07
KR20080027949A (en) 2008-03-28
CA2620139C (en) 2014-08-26
CN101273113A (en) 2008-09-24
EP1917328A4 (en) 2012-02-01
CA2620139A1 (en) 2007-02-15

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