WO2003089102A2 - Solid/liquid separation system for multiphase converters - Google Patents
Solid/liquid separation system for multiphase converters Download PDFInfo
- Publication number
- WO2003089102A2 WO2003089102A2 PCT/US2003/011544 US0311544W WO03089102A2 WO 2003089102 A2 WO2003089102 A2 WO 2003089102A2 US 0311544 W US0311544 W US 0311544W WO 03089102 A2 WO03089102 A2 WO 03089102A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- slurry
- linear velocity
- chamber
- substrate
- cake
- Prior art date
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 33
- 239000007787 solid Substances 0.000 title abstract description 31
- 238000000926 separation method Methods 0.000 title abstract description 30
- 239000002002 slurry Substances 0.000 claims abstract description 251
- 238000000034 method Methods 0.000 claims abstract description 82
- 239000000758 substrate Substances 0.000 claims abstract description 78
- 238000001914 filtration Methods 0.000 claims abstract description 67
- 239000012065 filter cake Substances 0.000 claims abstract description 39
- 230000001105 regulatory effect Effects 0.000 claims abstract description 32
- 230000000694 effects Effects 0.000 claims abstract description 12
- 238000013461 design Methods 0.000 claims abstract description 8
- 239000000706 filtrate Substances 0.000 claims description 102
- 239000002245 particle Substances 0.000 claims description 35
- 239000003054 catalyst Substances 0.000 claims description 24
- 230000004907 flux Effects 0.000 claims description 24
- 239000007790 solid phase Substances 0.000 claims description 24
- 239000007791 liquid phase Substances 0.000 claims description 15
- 230000007423 decrease Effects 0.000 claims description 14
- 230000015572 biosynthetic process Effects 0.000 claims description 13
- 238000003786 synthesis reaction Methods 0.000 claims description 10
- 229910052751 metal Inorganic materials 0.000 claims description 9
- 239000002184 metal Substances 0.000 claims description 9
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 8
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 8
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 8
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 8
- 229930195733 hydrocarbon Natural products 0.000 claims description 8
- 150000002430 hydrocarbons Chemical class 0.000 claims description 8
- 230000035699 permeability Effects 0.000 claims description 8
- 230000001419 dependent effect Effects 0.000 claims description 6
- 239000012528 membrane Substances 0.000 claims description 6
- 229910017052 cobalt Inorganic materials 0.000 claims description 5
- 239000010941 cobalt Substances 0.000 claims description 5
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 5
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 claims description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 4
- 229910052742 iron Inorganic materials 0.000 claims description 4
- 239000012466 permeate Substances 0.000 claims description 4
- 229910052707 ruthenium Inorganic materials 0.000 claims description 4
- 239000000377 silicon dioxide Substances 0.000 claims description 4
- 230000001276 controlling effect Effects 0.000 claims description 3
- 239000000835 fiber Substances 0.000 claims description 2
- 239000000047 product Substances 0.000 abstract description 12
- 239000012263 liquid product Substances 0.000 abstract description 6
- 239000012530 fluid Substances 0.000 abstract description 4
- 239000001993 wax Substances 0.000 description 14
- 239000007789 gas Substances 0.000 description 13
- 238000002156 mixing Methods 0.000 description 7
- 238000002474 experimental method Methods 0.000 description 5
- 238000000429 assembly Methods 0.000 description 4
- 230000000712 assembly Effects 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 3
- 229910002091 carbon monoxide Inorganic materials 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000376 reactant Substances 0.000 description 3
- 239000011949 solid catalyst Substances 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- 238000009295 crossflow filtration Methods 0.000 description 2
- DIOQZVSQGTUSAI-UHFFFAOYSA-N decane Chemical compound CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000007872 degassing Methods 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 230000000153 supplemental effect Effects 0.000 description 2
- 241000982035 Sparattosyce Species 0.000 description 1
- -1 aliphatic alcohols Chemical class 0.000 description 1
- 238000011001 backwashing Methods 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000009903 catalytic hydrogenation reaction Methods 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 238000007885 magnetic separation Methods 0.000 description 1
- 239000006148 magnetic separator Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000011165 process development Methods 0.000 description 1
- 238000011027 product recovery Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 239000011882 ultra-fine particle Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D37/00—Processes of filtration
- B01D37/02—Precoating the filter medium; Addition of filter aids to the liquid being filtered
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/11—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with bag, cage, hose, tube, sleeve or like filtering elements
- B01D29/13—Supported filter elements
- B01D29/15—Supported filter elements arranged for inward flow filtration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/60—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor integrally combined with devices for controlling the filtration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D37/00—Processes of filtration
- B01D37/04—Controlling the filtration
- B01D37/043—Controlling the filtration by flow measuring
Abstract
Description
Claims
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP03724031A EP1495093A2 (en) | 2002-04-16 | 2003-04-16 | Solid/liquid separation system for multiphase converters |
CA002482057A CA2482057A1 (en) | 2002-04-16 | 2003-04-16 | Solid/liquid separation system for multiphase converters |
AU2003230924A AU2003230924A1 (en) | 2002-04-16 | 2003-04-16 | Solid/liquid separation system for multiphase converters |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US37296102P | 2002-04-16 | 2002-04-16 | |
US60/372,961 | 2002-04-16 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2003089102A2 true WO2003089102A2 (en) | 2003-10-30 |
WO2003089102A3 WO2003089102A3 (en) | 2004-07-01 |
Family
ID=29250938
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2003/011544 WO2003089102A2 (en) | 2002-04-16 | 2003-04-16 | Solid/liquid separation system for multiphase converters |
PCT/US2003/011662 WO2003089103A2 (en) | 2002-04-16 | 2003-04-16 | Optimized solid/liquid separation system for multiphase converters |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2003/011662 WO2003089103A2 (en) | 2002-04-16 | 2003-04-16 | Optimized solid/liquid separation system for multiphase converters |
Country Status (6)
Country | Link |
---|---|
US (2) | US6929754B2 (en) |
EP (2) | EP1495093A2 (en) |
AU (2) | AU2003223624A1 (en) |
CA (2) | CA2482062A1 (en) |
WO (2) | WO2003089102A2 (en) |
ZA (2) | ZA200407224B (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7378452B2 (en) | 2005-12-28 | 2008-05-27 | Exxonmobil Research And Engineering Company | Filtration system for slurry hydrocarbon synthesis process using both small and large pore filter elements |
Families Citing this family (28)
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---|---|---|---|---|
ITMI20030969A1 (en) * | 2003-05-15 | 2004-11-16 | Enitecnologie Spa | PROCEDURE FOR THE CONTINUOUS PRODUCTION OF HYDROCARBONS FROM SYNTHESIS GAS IN SUSPENSION REACTORS AND FOR THE SEPARATION OF THE LIQUID PHASE PRODUCED FROM THE SOLID PHASE. |
ITMI20031029A1 (en) * | 2003-05-22 | 2004-11-23 | Enitecnologie Spa | PROCEDURES FOR THE CONTINUOUS PRODUCTION OF HYDROCARBONS FROM SYNTHESIS GAS. |
US7375143B2 (en) * | 2004-11-22 | 2008-05-20 | Conocophillips Company | Catalyst recover from a slurry |
US20060111232A1 (en) * | 2004-11-22 | 2006-05-25 | Conocophillips Company | Multi-staged wax displacement process for catalyst recovery from a slurry |
DE202005021612U1 (en) * | 2005-04-04 | 2008-11-27 | Wehrle Umwelt Gmbh | Plant for carrying out processes for the separation of ingredients from a flowable mixture of substances |
EP1940540B1 (en) * | 2005-10-04 | 2009-09-16 | The Petroleum Oil and Gas Corporation of South Africa (Pty) Ltd. | Filtration method |
WO2007060228A1 (en) * | 2005-11-28 | 2007-05-31 | Shell Internationale Research Maatschappij B.V. | A method for receiving fluid from a natural gas pipeline |
US8057744B2 (en) * | 2005-12-14 | 2011-11-15 | Nippon Steel Engineering Co., Ltd. | Bubble column-type Fischer-Tropsch synthesis slurry bed reaction system |
US7562588B2 (en) * | 2006-04-27 | 2009-07-21 | Delphi Technologies, Inc. | Method and apparatus for controlling mass flow rate of recycled anode tail gas in solid oxide fuel cell system |
CN100443155C (en) * | 2006-05-31 | 2008-12-17 | 中国石油化工股份有限公司 | Slurry bed circulatory flow reactor and uses thereof |
DE102007056170A1 (en) * | 2006-12-28 | 2008-11-06 | Dominik Peus | Substance or fuel for producing energy from biomass, is manufactured from biomass, which has higher carbon portion in comparison to raw material concerning percentaged mass portion of elements |
AU2008256233B2 (en) | 2007-05-28 | 2012-02-02 | The Petroleum Oil And Gas Corporation Of South Africa (Pty) Ltd | Removal of fine particles from a Fischer Tropsch stream |
US8442003B2 (en) * | 2007-09-06 | 2013-05-14 | Qualcomm Incorporated | Routing in a mesh network |
US8871096B2 (en) | 2007-09-10 | 2014-10-28 | Res Usa, Llc | Magnetic separation combined with dynamic settling for fischer-tropsch processes |
FR2922464B1 (en) | 2007-10-18 | 2010-06-04 | Inst Francais Du Petrole | DEVICE FOR SEPARATING A FINALLY DIVIDED SOLID IN SUSPENSION IN A VISCOUS LIQUID |
US7737068B2 (en) * | 2007-12-20 | 2010-06-15 | Chevron U.S.A. Inc. | Conversion of fine catalyst into coke-like material |
US7790646B2 (en) * | 2007-12-20 | 2010-09-07 | Chevron U.S.A. Inc. | Conversion of fine catalyst into coke-like material |
US8765622B2 (en) * | 2007-12-20 | 2014-07-01 | Chevron U.S.A. Inc. | Recovery of slurry unsupported catalyst |
US20090159495A1 (en) * | 2007-12-20 | 2009-06-25 | Chevron U.S.A. Inc. | Heavy oil conversion |
US8722556B2 (en) * | 2007-12-20 | 2014-05-13 | Chevron U.S.A. Inc. | Recovery of slurry unsupported catalyst |
MY160609A (en) * | 2008-09-30 | 2017-03-15 | Japan Oil Gas & Metals Jogmec | System for separating catalyst |
US20100084350A1 (en) | 2008-10-06 | 2010-04-08 | Jing Liu | Systems and Methods for Continuous Multiphase Reaction and Separation |
US8778178B2 (en) * | 2008-10-13 | 2014-07-15 | Rentech, Inc. | Integrated multi-step solid/liquid separation system for Fischer-Tropsch processes |
US8022109B2 (en) | 2008-12-23 | 2011-09-20 | Exxonmobil Research And Engineering Company | Product filtration system for slurry reactors |
EP2437877B1 (en) * | 2009-06-05 | 2017-12-20 | Solvay Sa | Process for separating liquid from a multiphase mixture |
KR101210397B1 (en) * | 2010-09-17 | 2012-12-10 | 한국화학연구원 | Catalyst/Wax separation device in a slurry phase Fischer-Tropsch synthesis reactor system |
CN105036298B (en) * | 2011-04-05 | 2018-06-15 | 格兰富控股联合股份公司 | For the method and system filtered and cake layer is formed |
CN105802657A (en) * | 2016-05-16 | 2016-07-27 | 中国石油大学(华东) | Catalytic cracking slurry oil solid content removal method |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4530764A (en) * | 1983-07-18 | 1985-07-23 | Occidental Research Corporation | Densification of phosphatic wastes and phosphoric acid slimes and solvent recovery |
US5919721A (en) * | 1991-09-30 | 1999-07-06 | Exxon Chemical Patents Inc | Microfiltration of zeolites |
Family Cites Families (26)
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US278880A (en) * | 1883-06-05 | Car-coupling | ||
US559849A (en) * | 1896-05-12 | Wire fence | ||
US544006A (en) * | 1895-08-06 | Chuck for machine-tools | ||
US2738880A (en) | 1948-12-20 | 1956-03-20 | Phillips Petroleum Co | Apparatus for separating components of an organic mixture |
US4605678A (en) * | 1984-03-12 | 1986-08-12 | Mobil Oil Corporation | Separation of catalyst from slurry bubble column wax and catalyst recycle |
GB9203959D0 (en) | 1992-02-25 | 1992-04-08 | Norske Stats Oljeselskap | Method of conducting catalytic converter multi-phase reaction |
GB9203958D0 (en) * | 1992-02-25 | 1992-04-08 | Norske Stats Oljeselskap | Catalytic multi-phase reactor |
US5599849A (en) * | 1993-01-27 | 1997-02-04 | Sasol Chemical Industries (Proprietary) Limited | Process for producing liquid and, optionally, gaseous products from gaseous reactants |
US6069179A (en) | 1993-02-24 | 2000-05-30 | Den Norske Stats Oljeselskap As | Method of conducting catalytic converter multi-phase reaction |
US5527473A (en) | 1993-07-15 | 1996-06-18 | Ackerman; Carl D. | Process for performing reactions in a liquid-solid catalyst slurry |
GB2281224B (en) | 1993-08-24 | 1998-02-11 | Norske Stats Oljeselskap | Solid/liquid slurry treatment apparatus and catalytic multi-phase reactor |
US6114399A (en) * | 1993-10-27 | 2000-09-05 | North Carolina State University | Methods and apparatus for separating Fischer-Tropsch catalysts from liquid hydrocarbon product |
JPH0899021A (en) * | 1994-09-29 | 1996-04-16 | Yuasa Corp | Method for operation of filter module |
US5827903A (en) | 1996-01-31 | 1998-10-27 | The United States Of America As Represented By The Department Of Energy | Separation of catalyst from Fischer-Tropsch slurry |
US5900159A (en) * | 1996-02-29 | 1999-05-04 | Shell Oil Company | Method for separating liquid from a slurry |
US5948383A (en) * | 1997-03-26 | 1999-09-07 | Engelhard Corporation | Hybrid zeolite-silica compositions |
US5962537A (en) * | 1997-05-06 | 1999-10-05 | Exxon Research And Engineering Co | Multizone downcomer for slurry hydrocarbon syntheses process |
US5811469A (en) * | 1997-05-06 | 1998-09-22 | Exxon Research And Engineering Company | Slurry hydrocarbon synthesis with downcomer fed product filtration (LAW552) |
US5770629A (en) | 1997-05-16 | 1998-06-23 | Exxon Research & Engineering Company | Slurry hydrocarbon synthesis with external product filtration |
US6068760A (en) | 1997-08-08 | 2000-05-30 | Rentech, Inc. | Catalyst/wax separation device for slurry Fischer-Tropsch reactor |
ITMI980865A1 (en) * | 1998-04-23 | 1999-10-23 | Eniricerche S P A Ora Enitecno | PROCEDURE FOR THE PREPARATION OF HYDROCARBONS FROM SYNTHESIS GAS |
EP1089956B1 (en) | 1998-06-11 | 2003-11-05 | Sasol Technology (Proprietary) Limited | Production of hydrocarbons |
US6344490B1 (en) | 1999-01-22 | 2002-02-05 | Exxon Research And Engineering Company | Removable filter for slurry hydrocarbon synthesis process |
EG22489A (en) * | 1999-02-05 | 2003-02-26 | Sasol Technology | Process for producing liquid and optionally gaseous products from gaseous reactants |
AR034670A1 (en) | 2001-07-03 | 2004-03-03 | Shell Int Research | PROCEDURE FOR THE PREPARATION OF LIQUID HYDROCARBONS |
US6833078B2 (en) * | 2002-09-13 | 2004-12-21 | Conocophillips Company | Solid-liquid separation system |
-
2003
- 2003-04-16 CA CA002482062A patent/CA2482062A1/en not_active Abandoned
- 2003-04-16 AU AU2003223624A patent/AU2003223624A1/en not_active Abandoned
- 2003-04-16 WO PCT/US2003/011544 patent/WO2003089102A2/en not_active Application Discontinuation
- 2003-04-16 ZA ZA200407224A patent/ZA200407224B/en unknown
- 2003-04-16 EP EP03724031A patent/EP1495093A2/en not_active Withdrawn
- 2003-04-16 WO PCT/US2003/011662 patent/WO2003089103A2/en not_active Application Discontinuation
- 2003-04-16 US US10/414,636 patent/US6929754B2/en not_active Expired - Fee Related
- 2003-04-16 EP EP03719763A patent/EP1494783A2/en not_active Withdrawn
- 2003-04-16 AU AU2003230924A patent/AU2003230924A1/en not_active Abandoned
- 2003-04-16 US US10/417,307 patent/US6887390B2/en not_active Expired - Fee Related
- 2003-04-16 CA CA002482057A patent/CA2482057A1/en not_active Abandoned
- 2003-04-16 ZA ZA200407368A patent/ZA200407368B/en unknown
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4530764A (en) * | 1983-07-18 | 1985-07-23 | Occidental Research Corporation | Densification of phosphatic wastes and phosphoric acid slimes and solvent recovery |
US5919721A (en) * | 1991-09-30 | 1999-07-06 | Exxon Chemical Patents Inc | Microfiltration of zeolites |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7378452B2 (en) | 2005-12-28 | 2008-05-27 | Exxonmobil Research And Engineering Company | Filtration system for slurry hydrocarbon synthesis process using both small and large pore filter elements |
Also Published As
Publication number | Publication date |
---|---|
US6929754B2 (en) | 2005-08-16 |
CA2482057A1 (en) | 2003-10-30 |
EP1495093A2 (en) | 2005-01-12 |
CA2482062A1 (en) | 2003-10-30 |
ZA200407224B (en) | 2006-02-22 |
EP1494783A2 (en) | 2005-01-12 |
ZA200407368B (en) | 2006-02-22 |
US20050027021A1 (en) | 2005-02-03 |
WO2003089103A3 (en) | 2004-03-04 |
AU2003230924A1 (en) | 2003-11-03 |
WO2003089102A3 (en) | 2004-07-01 |
US6887390B2 (en) | 2005-05-03 |
AU2003223624A1 (en) | 2003-11-03 |
US20030232894A1 (en) | 2003-12-18 |
WO2003089103A2 (en) | 2003-10-30 |
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