WO2001042615A2 - Drill rod - Google Patents
Drill rod Download PDFInfo
- Publication number
- WO2001042615A2 WO2001042615A2 PCT/US2000/042723 US0042723W WO0142615A2 WO 2001042615 A2 WO2001042615 A2 WO 2001042615A2 US 0042723 W US0042723 W US 0042723W WO 0142615 A2 WO0142615 A2 WO 0142615A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- rod
- threaded portion
- drill rod
- mating
- section
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
- C21D9/22—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for drills; for milling cutters; for machine cutting tools
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23P—METAL-WORKING NOT OTHERWISE PROVIDED FOR; COMBINED OPERATIONS; UNIVERSAL MACHINE TOOLS
- B23P15/00—Making specific metal objects by operations not covered by a single other subclass or a group in this subclass
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B17/00—Drilling rods or pipes; Flexible drill strings; Kellies; Drill collars; Sucker rods; Cables; Casings; Tubings
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B17/00—Drilling rods or pipes; Flexible drill strings; Kellies; Drill collars; Sucker rods; Cables; Casings; Tubings
- E21B17/02—Couplings; joints
- E21B17/04—Couplings; joints between rod or the like and bit or between rod and rod or the like
- E21B17/042—Threaded
- E21B17/0426—Threaded with a threaded cylindrical portion, e.g. for percussion rods
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D2221/00—Treating localised areas of an article
- C21D2221/01—End parts (e.g. leading, trailing end)
-
- C—CHEMISTRY; METALLURGY
- C21—METALLURGY OF IRON
- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
- C21D9/00—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
- C21D9/50—Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for welded joints
Definitions
- the present invention relates to rock drilling equipment, and more particularly to drill rod used for rock drilling operations.
- Speed rods 1 typically include a first section 2 having an externally-threaded rod portion 3 located at a first outer end 4 of the rod 1, referred to as the "male” end 4, and a second section 5 connected to the first section 2 and having a threaded hole 6 extending into a second, opposing outer end 7, referred to as the "female" end 7.
- the female end 7 has an outside diameter d f that is larger than the outside diameter d m of the male end, and is preferably sufficiently larger such that the threaded hole 6 is configured to threadably engage with the threaded portion 3 of the male end 4 of another speed rod 1 (only one shown).
- a drill string (not depicted) having a desired number of speed rods 1 may be easily constructed by threadably connecting the male end 4 of each rod 1 with the female end 7 of an adjacent rod 1.
- each speed rod 1 has a through bore hole or interior passage 8 extending along a central longitudinal axis 9 of the rod 1 between the opposing ends 4 and 7 and is used for flushing media through the drill rod 1.
- Speed drill rods 1 are typically fabricated by one of two known manufacturing techniques.
- the first method is to "upset forge" one end of a material rod that initially has a constant outside diameter and a longitudinal through bore.
- the material at the end being forged is displaced toward the other end and simultaneously displaced outwardly, such that the forged end increases in both outside and inside diameter, while the overall length of the rod decreases.
- the inside surface of the forged end is then finish machined and threaded to form a female end 7, and the other end is provided with external threads 3 on the outer surface to form a male end 4.
- Speed rods 1 formed by hot forging processes have several inherent problems or limitations resulting from the hot forging process.
- the interior bore or passage 8 of the drill rod 1 has a tendency to become reduced or close in during the forging process.
- the reduction in the interior passage 8 restricts the capability of flushing media through the rod 1.
- the inner surface of the drill rod 1, particularly at the forged (i.e., the female) end 7 has surface imperfections such as folded/lapped material or smeared material which act as stress concentrators. These stress concentrators cause the service life of the rods 1 to be greatly reduced.
- the forging process also creates sub-surface intergranular imperfections, such as discontinuous grain flow lines, in the material of the forged female end 7, particularly below the inner surface of the forged end 7. These intergranular imperfections result in a weak grain structure that is incapable of supporting the normal drilling forces required.
- the hot-forged female end 7 of the rod 1 usually has hard "scale” on the outer surfaces thereof and a core material hardness that is significantly increased by the hot-forging process. These two adverse effects make finish machining of the female end 8 more difficult and sometimes necessitates tempering of the female end 8 prior to finish machining. Furthermore, at portions of the drill rod 1 which are not finish machined, scale caused by the forging process is often present at the inner surfaces, which may lead to premature corrosion fatigue at such sections of the speed rod. In addition to the above-described problems, upset-forged speed rods 1 generally require lengthy process times throughout its manufacturing cycle, such the forging lead time from an outside vendor, and have a number of difficulties that typically arise throughout the manufacturing cycle.
- the drill rods 1 are difficult to handle during machining operations due to the fairly large overall length of the rods 1. Further, inconsistent machining tolerances are present in the finished rods 1 due to hard spots formed in the rod material during the forging process. Further, heat treatment of the rods 1 is difficult both due to the substantial overall length and weight of the rods 1, as well as the necessity of straightening rods which experience heat-induced bending, such straightening generally being performed by a vendor other than the one doing the heat treatment. Finally, it is also necessary to remove scale from the female threads 6 and inner surfaces of the rod 1. All of the process difficulties described above increase the costs of manufacturing the speed drill rods 1 by the upset-forging process.
- Another method of manufacturing the speed rods 1 is to inertia or friction weld together two rod sections 2, 5 and then finish machining the male and female portions of the welded together drill rod 1.
- inertia welding involves rotating one section (e.g., section 5) at a high speed and then displacing or pushing the other section (i.e., section 2) into the rotating section, creating substantial friction and heat, which melts material at the interface of the two sections 2 and 5. When the melted material later hardens, the two sections 2 and 5 are thus welded together.
- the male and female ends 4 and 7, respectively, of the rod 1 are then threaded, as discussed above, if not already provided with threads before welding.
- Speed drill rods 1 manufactured by inertia welding also typically have several problems or defects that arise from the inertia welding process.
- flash is typically present at the inertia welded joint at both the inner and outer surfaces of the drill rod 1.
- the flash is caused by rod material that flows, both inwardly and outwardly, during the inertia welding process.
- This flash restricts media flushing capability of the rod 1 and acts as stress concentrators at the inside and outside diameters of the rod, resulting in a greatly reduced service life of the rod. Therefore, the flash must be removed by appropriate means (e.g., grinding) in order to make the sections of the rod joint as smooth as possible in order to eliminate the stress concentrators.
- the joint section of the rod must be fully tempered.
- Speed rods 1 regardless of which of two above-described processes are used to manufacture a particular rod, are all typically heat-treated in the same manner.
- a rod 1 is first completely carburized such that a hardened casing is formed on generally all surfaces, as represented by thickened line sections in Fig. 1 , and then is tempered from end to end.
- Such heat treatment is believed to cause the mating threads 3 and 6 to be wear resistant, the outer or exterior surfaces of the rod 1 to be resistant to wearing- away caused by abrasion from rock cuttings during use of the drill string, and to also reduce any adverse material effects in the rod 1 that may have been created by heat during either the forging or welding processes.
- speed rod 1 is often subject to high bending loads caused by drilling feed pressure.
- the central body portion of the speed rod 1 often contacts and rubs against the material of a formation being drilled. Due to the increased hardness provided by the carburized casing, such bending loads and abrading contact with the material formation often causes friction cracks to appear on the outer surface of the central portion of the rod 1, which may lead to premature fracture of the speed rod 1.
- the above-described heat treatment typically raises the core hardness of the speed rods 1 so as to cause the rods 1 to be relatively fragile under normal drilling conditions.
- completely carburized drill rods 1 require a relatively long processing cycle and hence tend to generally expensive to heat treat.
- the carburization process can generally only be performed in a large furnace, increasing both the cost and processing time for treating the drill rod 1.
- the present invention provides an improved drill rod and a method of manufacturing an improved drill rod or drill string.
- the drill rod is made from two rod sections that serve to minimize the cost of manufacturing compared to the ordinarily long and inconvenient size of typical drill rod. Because of the convenient size of the two separate rod sections, they are separately heat treated and machined, thereby shortening the processing cycle and reducing the costs associated with their manufacture.
- the two rod sections can individually be more selectively hardened to provide hardened areas where strength is necessary and toughened sections where durability is required. This selective hardening provides a durable section that is less susceptible to cracks that eventually lead to fracture.
- the drill rod of the present invention provides simple manufacture, cost effectiveness, and a longer service life.
- the drill rod includes a first rod section and a second rod section that are welded together along their mating ends.
- the mating ends are heat treated to reduce the elevated hardness that is caused by welding.
- Both the first rod section and the second rod section each include an interior passage that extends between the free end to the mating end.
- a hardened externally threaded portion on the first rod section can be threaded into the separately hardened internally threaded portion in the interior passage of a second rod section of another drill rod.
- the first drill rod is preferably threaded into the other drill rod until the surface of an annular face on the free end of the first drill rod abuts against a mating shoulder of the second drill rod.
- Fig. 1 is a side plan view of a known speed drill rod
- Fig. 2 is a side plan view of an improved speed rod in accordance with the present invention.
- Fig. 3 is a side plan view of a first rod section of the improved drill rod; and Fig. 4 is an enlarged, side cross-sectional view of a second rod section of the improved drill rod.
- the present invention is an improved drill rod 10 having selectively hardened sections 12.
- the drill rod 10 basically comprises a first rod section 14 attached to a second rod section 16, preferably by an inertia welding process, so as to form a joint 13 between the two sections 14 and 16.
- Each rod section 14 and 16 is separately processed to form the hardened sections 12 of the rod 10 prior to being attached together, as discussed in further detail below.
- the second rod section 16, which provides the female end 10b of the rod 10 has an outside diameter D f that is substantially greater than an outside diameter D m of the first section 14, which provides the male end 10a of the rod 10, as for reasons described below.
- the first rod section 14 has a first, free end 14a (i.e., "free” when sections 14 and 16 are attached), a second, mating end 14b and a longitudinal bore hole 15 extending between the ends 14a and 14b.
- An externally threaded portion 18 is formed in the outer circumferential surface 14c of the rod section 14 and is disposed proximal the rod section free end 14a.
- a radial annular face or "rod contacting button” 20 is located at the free end 14a about one end of the bore-hole 15.
- the contacting button 20 provides a lead-in surface for mating with the female end 10b of another speed rod 10 (only one shown), as discussed below.
- the threaded portion 18 and the contacting button 20 are treated or processed to form the hardened sections 12 of the male end 10a of the drill rod 10, as represented by thickened line sections in Fig. 3.
- an induction coil (not shown) is disposed about the free end 14a of the rod section 14a such that magnetic energy is transferred from the coil to the rod material at the free end 14a, causing the rod material to become heated (as is known).
- the heated rod section is then quenched such that a hardened case is formed about the threaded portion 18 and the button 20.
- the portions 18, 20 of the first rod section 14 may be hardened by any other appropriate means, such as by selective carburization (although not preferred), as described below. Referring now to Figs.
- the second rod section 16 has a first, free end 16a, a second, mating end 16b, and a counter-bored hole 17 extending between the ends 16a and 16b.
- An internally threaded portion 22 is formed in the inner circumferential surface 16d that bounds the larger diameter section of the counter-bored hole 17 and extends axially from the free end 16a to a thread undercut or run-out groove 24.
- the internally threaded portion 22 is configured to threadably engage with the externally threaded portion 18 of another speed rod 10 (only one shown), to thereby connect together the two speed rods 10 (one shown).
- a radial "rod mating" shoulder 26 is formed at the intersection of the larger and smaller diameter sections of the counter-bored hole 17. The rod mating shoulder 26 provides an abutment surface for the rod contact button 20 at the male end 10a of another drill rod 10 when the two rods 10 are connected together.
- the internally threaded section 22, the thread run-out undercut 24 and the mating shoulder 26 are treated to form the selectively hardened sections 12 of the female end 10b of the rod 10, as represented by thickened line sections in Fig. 4.
- the portions 22, 24 and 26 of the second rod section 16 are heat-treated by "selective carburization" to form a hardened case at each section 22, 24 and 26.
- any rod portion where no hardening is desired is first coated with a substance referred to as "stop-off paint” and then the entire rod section 16 is heated in carbon rich environment. A hardened case is then formed at the non-coated surfaces of the rod section 16 but not at the painted surfaces.
- any other appropriate means for forming the selectively hardened sections 12 of the female end 10b may be used, such as for example, by induction heating the portions 22, 24 and 26 of the second rod section 16.
- the mating ends 14b, 16b of the two rod sections 14, 16, respectively are joined together to form the overall drill rod 10 (Fig. 2).
- the rod sections 14 and 16 are attached together using an inertia welding process, as described in the Background section of the present application, although any other appropriate process, such as for example, upset- forging (not preferred) may alternatively be used to join the rod sections 14 and 16.
- the joint 13 is preferably locally tempered by induction heating or by using a torch flame in order to reduce any elevated hardness in the material about the joint 13.
- the joint 13 is fully tempered (i.e., completely from the joint outer surface 13a to joint inner surface 13b) to prevent this portion of the rod 10 from being relatively fragile and susceptible to failure or fracture.
- tempering process is not appropriately performed such that only the weld-hardened sections (i.e., the joint 15 and the immediately adjacent material sections) are tempered, other, non-hardened sections of the rod 10 adjacent to the joint 15 may become tempered and the material reduced to unacceptable hardness levels.
- induction heating or torch flaming are preferred for tempering the joint 13 as these processes are capable of being appropriately controlled to limit the tempered regions as desired.
- the hardened sections 12 of the rod 10 preferably have a hardness, as measured on the well-known Rockwell "C" scale, of at least Re 50, and hardnesses within the range of about Re 55 to about Re 60 have been found to provide suitable protection to the portions 18, 20, 22, 24 and 26 of the drill rod 10. Further, the remaining portions/sections of the rod 10 preferably have a hardness within the range of about Re 30 to about Re 42.
- the drill rod 10 is fabricated of the type of steel commonly referred to as "chrome-mo ly steel", although any other appropriate grade of steel or steel alloy or another type of metal/metal alloy may alternatively be used to fabricate the improved rod 10.
- the improved rod 10 By hardening only certain sections 12 of the drill rod 10 and leaving the remaining rod sections in a non-hardened state, the improved rod 10 is able to resist impact damage and material wearing where such damage/wear is likely to occur (and significantly affect the functionality of the rod 10, as discussed below) while maintaining the overall rod 10 in a relatively ductile state. More specifically, the threaded portions 18 and 22, which mate with the corresponding threaded portions 22, 18, respectively, of another speed rod 10
- the ductility of the rod 10 is sufficiently high to make the rod 10 less prone to failure due to bending, shear or torsional stresses compared with a fully carburized rod 1.
- the exposed outer or exterior surfaces 14c, 16c (i.e., when connected in a drill string) of the drill rod 10 being non-hardened (Fig. 2), these surfaces are less likely to fail due to cracks caused by friction generated by abrasive contact with the cut-out walls of a drilling formation or with drill centralizers.
- the crack is likely to "rub off' due to rod material around the crack abrading away by the rubbing contact with the formation surfaces.
- the improved rod 10 of the present invention has a number of advantages over previously known speed drill rod 1. As discussed above, selective hardening of certain sections 12 provides the benefits of hardening where needed while preserving the ductility of remainder of the rod 10. Also, by hardening portions of the individual rod sections 14, 16 in separate processes prior to attachment, it is much easier to handle the individual sections 14, 16 as compared to the entire drill rod 10.
- the improved speed rod 10 is less time-consuming and more cost effective to produce than the previously known, fully carburized drill rod 1.
Abstract
Description
Claims
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AU45225/01A AU4522501A (en) | 1999-12-10 | 2000-12-08 | Drill rod having selectively hardened sections |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US17016999P | 1999-12-10 | 1999-12-10 | |
US60/170,169 | 1999-12-10 |
Publications (2)
Publication Number | Publication Date |
---|---|
WO2001042615A2 true WO2001042615A2 (en) | 2001-06-14 |
WO2001042615A3 WO2001042615A3 (en) | 2002-01-24 |
Family
ID=22618837
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
PCT/US2000/042723 WO2001042615A2 (en) | 1999-12-10 | 2000-12-08 | Drill rod |
Country Status (2)
Country | Link |
---|---|
AU (1) | AU4522501A (en) |
WO (1) | WO2001042615A2 (en) |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2004029403A1 (en) | 2002-09-24 | 2004-04-08 | Sandvik Ab | Drill rod and method in order to manufacture the same |
WO2004101948A1 (en) * | 2003-05-16 | 2004-11-25 | Atlas Copco Secoroc Ab | A connection rod for rock drilling and a method of producing the same. |
CN103132924A (en) * | 2013-01-30 | 2013-06-05 | 陈伟琛 | Petroleum drilling tool for surface hardening |
CN107190129A (en) * | 2017-06-09 | 2017-09-22 | 贵州高峰石油机械股份有限公司 | A kind of Technology for Heating Processing of the solid drill steel of structural alloy steel |
AU2013205904B2 (en) * | 2012-05-17 | 2017-12-07 | Woodstock Percussion Pty Ltd | Full Strength Threaded Bar |
EP2845993B1 (en) * | 2013-09-09 | 2018-01-10 | Sandvik Intellectual Property AB | Energy transmission efficient percussive drill string coupling |
CN110170801A (en) * | 2019-06-05 | 2019-08-27 | 刘艺纯 | Impact the manufacturing method of screw thread drill steel |
CN111975296A (en) * | 2020-08-11 | 2020-11-24 | 杭州锐健医疗股份有限公司 | Machining method of drill guide with eccentric teeth in knee joint operation |
CN112756910A (en) * | 2020-12-25 | 2021-05-07 | 中煤科工集团西安研究院有限公司 | Winding device and method for welding type multi-head spiral drill rod |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110052794A (en) * | 2019-06-05 | 2019-07-26 | 刘艺纯 | The manufacturing method of bit shank |
Citations (7)
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---|---|---|---|---|
US3484122A (en) * | 1968-01-12 | 1969-12-16 | Herman J Schellstede | Drill pipe protector and method of constructing the same |
US3773359A (en) * | 1971-06-24 | 1973-11-20 | Smith International | Intermediate drill stem |
US3784238A (en) * | 1971-05-17 | 1974-01-08 | Smith International | Intermediate drill stem |
US4509777A (en) * | 1982-11-01 | 1985-04-09 | Dril-Quip Inc. | Weld-on casing connector |
US5919578A (en) * | 1996-01-22 | 1999-07-06 | Sandvik Ab | Friction welded product and method for manufacturing thereof |
US5988301A (en) * | 1997-06-20 | 1999-11-23 | Sandvik Ab | Drill rod and method for its manufacture |
US6095266A (en) * | 1996-06-20 | 2000-08-01 | Sandvik Ab | Drill rod and method for its manufacturer |
-
2000
- 2000-12-08 AU AU45225/01A patent/AU4522501A/en not_active Abandoned
- 2000-12-08 WO PCT/US2000/042723 patent/WO2001042615A2/en active Application Filing
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3484122A (en) * | 1968-01-12 | 1969-12-16 | Herman J Schellstede | Drill pipe protector and method of constructing the same |
US3784238A (en) * | 1971-05-17 | 1974-01-08 | Smith International | Intermediate drill stem |
US3773359A (en) * | 1971-06-24 | 1973-11-20 | Smith International | Intermediate drill stem |
US4509777A (en) * | 1982-11-01 | 1985-04-09 | Dril-Quip Inc. | Weld-on casing connector |
US5919578A (en) * | 1996-01-22 | 1999-07-06 | Sandvik Ab | Friction welded product and method for manufacturing thereof |
US6095266A (en) * | 1996-06-20 | 2000-08-01 | Sandvik Ab | Drill rod and method for its manufacturer |
US5988301A (en) * | 1997-06-20 | 1999-11-23 | Sandvik Ab | Drill rod and method for its manufacture |
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2004029403A1 (en) | 2002-09-24 | 2004-04-08 | Sandvik Ab | Drill rod and method in order to manufacture the same |
US7571779B2 (en) | 2002-09-24 | 2009-08-11 | Sandvik Intellectual Property Aktiebolag | Drill rod and method of manufacture thereof |
EP2796573A1 (en) | 2002-09-24 | 2014-10-29 | Sandvik Intellectual Property AB | Drill rod and method in order to manufacture the same |
WO2004101948A1 (en) * | 2003-05-16 | 2004-11-25 | Atlas Copco Secoroc Ab | A connection rod for rock drilling and a method of producing the same. |
CN100432368C (en) * | 2003-05-16 | 2008-11-12 | 阿特拉斯·科普科塞科罗克股份公司 | Connection rod and method for production thereof |
AU2013205904B2 (en) * | 2012-05-17 | 2017-12-07 | Woodstock Percussion Pty Ltd | Full Strength Threaded Bar |
CN103132924A (en) * | 2013-01-30 | 2013-06-05 | 陈伟琛 | Petroleum drilling tool for surface hardening |
EP2845993B1 (en) * | 2013-09-09 | 2018-01-10 | Sandvik Intellectual Property AB | Energy transmission efficient percussive drill string coupling |
CN107190129A (en) * | 2017-06-09 | 2017-09-22 | 贵州高峰石油机械股份有限公司 | A kind of Technology for Heating Processing of the solid drill steel of structural alloy steel |
CN110170801A (en) * | 2019-06-05 | 2019-08-27 | 刘艺纯 | Impact the manufacturing method of screw thread drill steel |
CN111975296A (en) * | 2020-08-11 | 2020-11-24 | 杭州锐健医疗股份有限公司 | Machining method of drill guide with eccentric teeth in knee joint operation |
CN112756910A (en) * | 2020-12-25 | 2021-05-07 | 中煤科工集团西安研究院有限公司 | Winding device and method for welding type multi-head spiral drill rod |
Also Published As
Publication number | Publication date |
---|---|
AU4522501A (en) | 2001-06-18 |
WO2001042615A3 (en) | 2002-01-24 |
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