EP1122299A2 - Laundry composition - Google Patents
Laundry composition Download PDFInfo
- Publication number
- EP1122299A2 EP1122299A2 EP00311581A EP00311581A EP1122299A2 EP 1122299 A2 EP1122299 A2 EP 1122299A2 EP 00311581 A EP00311581 A EP 00311581A EP 00311581 A EP00311581 A EP 00311581A EP 1122299 A2 EP1122299 A2 EP 1122299A2
- Authority
- EP
- European Patent Office
- Prior art keywords
- particles
- composition
- liquid
- agent
- dye
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0008—Detergent materials or soaps characterised by their shape or physical properties aqueous liquid non soap compositions
- C11D17/0013—Liquid compositions with insoluble particles in suspension
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0039—Coated compositions or coated components in the compositions, (micro)capsules
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3947—Liquid compositions
Definitions
- One preferred active ingredient within the particles is a dye-transfer inhibitor.
- the particle cores were made by melting the stearic acid mixed with the Na HEDP (in powder form), and then spray chilling.
- the resultant solid cores were then coated using commercially available Glatt technology.
- the plasticizer and the acrylic precursors were dissolved in 60% acetone/40% isopropanol (v:v).
- the concentration of the materials in the solvent was 10% by weight.
- the cores were coated in a vertical fluid bed, the acrylic material being polymerised in situ.
- the resulting particles having a mean size (diameter) of about 1.5 mm and a density of about 1 g/cm 3 , were incorporated in two acidic liquid bleach formulations E1 (containing P1 particles) and E2 (containing P2 particles), set out below.
Abstract
Description
and wherein the particles are stable in the acidic liquid but dissolve or disperse under alkaline washing conditions.
Cellulose acetate phthalate (Cellacephate®, CAP), vinyl acetate crotonic acid copolymer (Luviset®), methacrylic acid, (meth)acrylic acid ester copolymer (Eudragit®) and hydroxypropyl methylcellulose phthalate.
Composition | P1 | P2 |
% | % | |
Stearic acid (carrier) | 60 | 50 |
Na HEDP (chelating agent) | 20 | 15 |
EUDRAGIT S100 | 15 | 25 |
Diisopropyl adipate (plasticizer for coating) | 5 | 10 |
Composition | E1 | E2 | V1 |
% | % | % | |
Hydrogen peroxide | 6.50 | 6.50 | 6.50 |
LIALET 125/5 | 7.00 | 7.00 | 7.00 |
Na HEDP | 0.12 | 0.12 | 0.7 |
Particles | 4.37 | 5.00 | 0 |
POLYGEL DA | 0.20 | 0.20 | 0.20 |
Perfume | 0.20 | 0.20 | 0.20 |
Pigment | 0.001 | 0.001 | 0 |
Deionised water | to 100 | to 100 | To 100 |
Viscosity (cps, at 20°C) | 500-1000 | 500-1000 | 1000-1500 |
PH | 4.2 | 4.2 | 4.2 |
Color/fabric | Evaluation type | Composition | Delta | ||
E1 | E2 | V1 | |||
Sirius Blue CLB on cotton | Visual | 2.0 | 3.0 | + 1.0 | |
Instrumental | 6.0 | 9.6 | + 3.6 | ||
Sirius Blue CLB on viscose | Visual | 2.0 | 3.0 | + 1.0 | |
Instrumental | 7.4 | 10.7 | + 3.3 | ||
Sirius Red SLR on cotton | Visual | 2.5 | 3.0 | + 0.5 | |
Instrumental | 5.4 | 11.5 | + 1.8 | ||
Sirius Red SLR on viscose | Visual | 2.0 | 3.0 | + 1.0 | |
Instrumental | 5.4 | 5.8 | + 0.4 | ||
Sirius Yellow SLG on cotton | Visual | 2.5 | 3.5 | + 1.0 | |
Instrumental | 11.4 | 14.0 | +2.6 | ||
Sirius Yellow on viscose | Visual | 2.0 | 3.0 | + 1.0 | |
Instrumental | 8.2 | 9.7 | + 1.5 |
Stearic acid | 81% |
Titania powder (rutile, sub-micron) | 9% |
EUDRAGIT copolymer | 9% |
Diisopropyl adipate | 1% |
Ingredients | % |
Hydrogen peroxide | 6.5% |
Na HEDP | 0.2% |
LIALET 125/5 | 7.0% |
POLYGEL DA | 0.2% |
Blue pigment | 0.001% |
Phthalocyanine green dye | 0.0002% |
Perfume | 0.27% |
Particles | 0.2% |
Sodium hydroxide | to pH 4.3 |
Deionised water | to 100% |
Ingredients | % |
Hydrogen peroxide | 6.5% |
LIALET 125/5 | 7.0% |
VERSENEX 80E | 0.3% |
POLYGEL DA | 0.3% |
Blue dye | 0.0005% |
Perfume | 0.27% |
Particles | 0.2% |
Sodium hydroxide | to pH 4.3 |
Deionised water | to 100% |
Ingredients | % |
Hydrogen peroxide | 6.5% |
LIALET 125/5 | 7.0% |
DETAREX | 0.12% |
POLYGEL DA | 0.3% |
Blue dye | 0.0005% |
Perfume | 0.27% |
Particles | 0.2% |
Sodium hydroxide | to pH 4.3 |
Deionised water | to 100% |
Ingredients | % |
Hydrogen peroxide | 6.5% |
LIALET 125/5 | 7.0% |
ACRILAM C20 | 0.2% |
POLYGEL DA | 0.20% |
OXY RITE | 0.15% |
Blue dye | 0.0005% |
Perfume | 0.27% |
Particles | 0.2% |
Sodium hydroxide | to pH 4.3 |
Deionised water | to 100% |
% PVNO in particles | Reflectance value - white part | Reflectance value -colored part |
0 (comparison) | 4.7 | 4.2 |
10 (composition E7) | 3.4 | 4.3 |
20 (composition E8) | 2.2 | 4.3 |
30 (composition E9) | 1.1 | 4.4 |
40 (composition E10) | 0.8 | 4.5 |
Ingredients | % |
Hydrogen peroxide | 6.5% |
LIALET 125/5 | 7.0% |
ACRILAM C20 | 0.3% |
POLYGEL DA | 0.2% |
Xanthan gum (stabiliser) | 0.05% |
Blue pigment | 0.001% |
Phthalocyanine green dye | 0.0002% |
Perfume | 0.27% |
Particles (see above) | 0.2% |
Sodium hydroxide | To pH 4.3 |
Deionised water | To 100% |
Viscosity: after 24 h at 20°C (cps) | 1400 | ||
After 6 days | 2°C | 1180 | All particles remain in homogenous suspension |
20°C | 1340 | ||
40°C | 1540 | ||
After 1 month | 2°C | 1120 | All particles remain in homogenous suspension |
20°C | 1340 | ||
40°C | 1650 | ||
After 2.5 months | 2°C | 1000 | All particles remain in homogenous suspension |
20°C | 1200 | ||
40°C | 1100 | ||
After 3 months | 2°C | 1130 | All particles remain in homogenous suspension |
20°C | 1380 | ||
40°C | 900 |
Claims (10)
- A laundry composition comprising:a) an acidic liquid containing hydrogen peroxide, andb) particles suspended in the liquid
and wherein the particles are stable in the acidic liquid but dissolve or disperse under alkaline washing conditions. - A composition as claimed in claim 1, wherein the core includes a chelating agent.
- A composition as claimed in claim 2, wherein the chelating agent comprises a compound selected from a phosphonate and a polyacetic derivative and a polyacrylic derivative.
- A composition as claimed in any preceding claim, wherein the core includes a dye-transfer inhibitor.
- A composition as claimed in any of claims 2 to 4, wherein the core additionally includes one or more compounds selected from an anti-fading agent, an anti-bacterial agent, a fabric softener, a transition metal compound and an optical brightener.
- A composition as claimed in any preceding claim, wherein the particles are of mean size 0.5 mm to 3 mm.
- A composition as claimed in any preceding claim, wherein the particles have a density which is within 0.2 g/cm3 of the density of the liquid.
- A composition as claimed in any preceding claim, wherein the liquid contains a nonionic surfactant.
- A composition as claimed in any preceding claim, wherein the liquid contains a chelating agent.
- A method of laundering fabrics, using a laundry detergent and, in addition, a composition as claimed in any preceding claim.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP20000311581 EP1122299B1 (en) | 1999-12-28 | 2000-12-22 | Laundry composition |
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP99125979 | 1999-12-28 | ||
EP99125979A EP1113069A1 (en) | 1999-12-28 | 1999-12-28 | Liquid peroxide bleaches comprising speckles in suspension |
EP20000311581 EP1122299B1 (en) | 1999-12-28 | 2000-12-22 | Laundry composition |
Publications (3)
Publication Number | Publication Date |
---|---|
EP1122299A2 true EP1122299A2 (en) | 2001-08-08 |
EP1122299A3 EP1122299A3 (en) | 2001-10-04 |
EP1122299B1 EP1122299B1 (en) | 2005-07-06 |
Family
ID=26073391
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP20000311581 Expired - Lifetime EP1122299B1 (en) | 1999-12-28 | 2000-12-22 | Laundry composition |
Country Status (1)
Country | Link |
---|---|
EP (1) | EP1122299B1 (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2009047745A2 (en) * | 2009-01-29 | 2009-04-16 | The Procter & Gamble Company | Encapsulates |
WO2009083941A2 (en) * | 2009-01-29 | 2009-07-09 | The Procter & Gamble Company | Encapsulates |
EP2208776A1 (en) * | 2009-01-16 | 2010-07-21 | The Procter and Gamble Company | Bleaching compositions containing perfume microcapsules |
WO2012164266A1 (en) * | 2011-05-27 | 2012-12-06 | Reckitt Benckiser N.V. | Composition |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0201958A1 (en) * | 1985-05-07 | 1986-11-20 | Akzo N.V. | Pourable detergent and bleach compositions |
US4642198A (en) * | 1984-05-01 | 1987-02-10 | Lever Brothers Company | Liquid bleaching compositions |
WO1987007292A1 (en) * | 1986-05-21 | 1987-12-03 | Novo Industri A/S | Coated detergent enzymes |
DE4040654A1 (en) * | 1990-12-19 | 1992-06-25 | Henkel Kgaa | GRANULES WITH COVERED BLEACH ACTIVATOR |
WO1995014077A1 (en) * | 1993-11-16 | 1995-05-26 | Warwick International Group Limited | Bleach activator compositions |
US5460743A (en) * | 1994-05-09 | 1995-10-24 | Lever Brothers Company, Division Of Conopco, Inc. | Liquid cleaning composition containing polyvinyl ether encapsulated particles |
US5641739A (en) * | 1995-05-01 | 1997-06-24 | The Procter & Gamble Company | Aqueous detergent compositions containing chelants which remain undissolved under acidic conditions |
DE29903534U1 (en) * | 1999-02-27 | 1999-06-17 | Henkel Kgaa | Peroxide-containing preparations with colorants in microcapsules |
DE19855346A1 (en) * | 1998-12-01 | 2000-06-08 | Henkel Kgaa | Preparations containing peroxide with stabilized optical brighteners |
-
2000
- 2000-12-22 EP EP20000311581 patent/EP1122299B1/en not_active Expired - Lifetime
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4642198A (en) * | 1984-05-01 | 1987-02-10 | Lever Brothers Company | Liquid bleaching compositions |
EP0201958A1 (en) * | 1985-05-07 | 1986-11-20 | Akzo N.V. | Pourable detergent and bleach compositions |
WO1987007292A1 (en) * | 1986-05-21 | 1987-12-03 | Novo Industri A/S | Coated detergent enzymes |
DE4040654A1 (en) * | 1990-12-19 | 1992-06-25 | Henkel Kgaa | GRANULES WITH COVERED BLEACH ACTIVATOR |
WO1995014077A1 (en) * | 1993-11-16 | 1995-05-26 | Warwick International Group Limited | Bleach activator compositions |
US5460743A (en) * | 1994-05-09 | 1995-10-24 | Lever Brothers Company, Division Of Conopco, Inc. | Liquid cleaning composition containing polyvinyl ether encapsulated particles |
US5641739A (en) * | 1995-05-01 | 1997-06-24 | The Procter & Gamble Company | Aqueous detergent compositions containing chelants which remain undissolved under acidic conditions |
DE19855346A1 (en) * | 1998-12-01 | 2000-06-08 | Henkel Kgaa | Preparations containing peroxide with stabilized optical brighteners |
DE29903534U1 (en) * | 1999-02-27 | 1999-06-17 | Henkel Kgaa | Peroxide-containing preparations with colorants in microcapsules |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2208776A1 (en) * | 2009-01-16 | 2010-07-21 | The Procter and Gamble Company | Bleaching compositions containing perfume microcapsules |
WO2010083125A1 (en) * | 2009-01-16 | 2010-07-22 | The Procter & Gamble Company | Bleaching compositions containing perfume microcapsules |
WO2009047745A2 (en) * | 2009-01-29 | 2009-04-16 | The Procter & Gamble Company | Encapsulates |
WO2009083941A2 (en) * | 2009-01-29 | 2009-07-09 | The Procter & Gamble Company | Encapsulates |
WO2009083941A3 (en) * | 2009-01-29 | 2009-12-10 | The Procter & Gamble Company | Encapsulates |
WO2009047745A3 (en) * | 2009-01-29 | 2009-12-10 | The Procter & Gamble Company | Encapsulates |
JP2012516371A (en) * | 2009-01-29 | 2012-07-19 | ザ プロクター アンド ギャンブル カンパニー | Inclusion body |
WO2012164266A1 (en) * | 2011-05-27 | 2012-12-06 | Reckitt Benckiser N.V. | Composition |
Also Published As
Publication number | Publication date |
---|---|
EP1122299B1 (en) | 2005-07-06 |
EP1122299A3 (en) | 2001-10-04 |
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