DE69905962D1 - Synthese von Triethylendiamin und Piperazine mit Hilfe von mit Silicium enthaltende Verbindungen modifizierten Zeolith Katalysatoren - Google Patents
Synthese von Triethylendiamin und Piperazine mit Hilfe von mit Silicium enthaltende Verbindungen modifizierten Zeolith KatalysatorenInfo
- Publication number
- DE69905962D1 DE69905962D1 DE69905962T DE69905962T DE69905962D1 DE 69905962 D1 DE69905962 D1 DE 69905962D1 DE 69905962 T DE69905962 T DE 69905962T DE 69905962 T DE69905962 T DE 69905962T DE 69905962 D1 DE69905962 D1 DE 69905962D1
- Authority
- DE
- Germany
- Prior art keywords
- piperazines
- triethylenediamine
- synthesis
- silicon
- containing compounds
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C211/00—Compounds containing amino groups bound to a carbon skeleton
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D295/00—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms
- C07D295/02—Heterocyclic compounds containing polymethylene-imine rings with at least five ring members, 3-azabicyclo [3.2.2] nonane, piperazine, morpholine or thiomorpholine rings, having only hydrogen atoms directly attached to the ring carbon atoms containing only hydrogen and carbon atoms in addition to the ring hetero elements
- C07D295/023—Preparation; Separation; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/04—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups
- C07C209/14—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups
- C07C209/16—Preparation of compounds containing amino groups bound to a carbon skeleton by substitution of functional groups by amino groups by substitution of hydroxy groups or of etherified or esterified hydroxy groups with formation of amino groups bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/64—Preparation of compounds containing amino groups bound to a carbon skeleton by disproportionation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
- C07D487/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains two hetero rings
- C07D487/08—Bridged systems
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US09/057,662 US6084096A (en) | 1998-04-09 | 1998-04-09 | Triethylenediamine and piperazine synthesis using zeolite catalysts modified with a silicon-containing compound |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69905962D1 true DE69905962D1 (de) | 2003-04-24 |
DE69905962T2 DE69905962T2 (de) | 2003-09-11 |
Family
ID=22011989
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69905962T Expired - Fee Related DE69905962T2 (de) | 1998-04-09 | 1999-04-08 | Synthese von Triethylendiamin und Piperazine mit Hilfe von mit Silicium enthaltende Verbindungen modifizierten Zeolith Katalysatoren |
Country Status (6)
Country | Link |
---|---|
US (1) | US6084096A (de) |
EP (1) | EP0952152B1 (de) |
JP (1) | JP3883326B2 (de) |
KR (1) | KR100322780B1 (de) |
CN (1) | CN1121400C (de) |
DE (1) | DE69905962T2 (de) |
Families Citing this family (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR100284936B1 (ko) * | 1998-12-31 | 2001-04-02 | 김충섭 | 촉매 활성 귀금속 담지 제올라이트계 탈질 촉매의 제조 방법 |
US6350874B1 (en) * | 1999-04-01 | 2002-02-26 | Tosoh Corporation | Method for producing triethylenediamines and piperazines |
DE19930736C2 (de) * | 1999-07-05 | 2001-07-05 | Performance Chemicals Handels | Verfahren zur Herstellung von Triethylendiamin unter Einsatz von Ethylendiamin |
US6403835B1 (en) | 1999-11-02 | 2002-06-11 | California Institute Of Technology | Acylation of an organic group over a zeolite |
JP4496633B2 (ja) * | 2000-09-29 | 2010-07-07 | 東ソー株式会社 | トリエチレンジアミン製造用成形体触媒とその製造法及びトリエチレンジアミンの製造方法 |
DE10061863A1 (de) * | 2000-12-12 | 2002-06-13 | Basf Ag | Verfahren zur Herstellung von Triethylendiamin (TEDA) |
US6864200B2 (en) * | 2001-01-23 | 2005-03-08 | Indian Petrochemicals Corporation Limited | Selectivated metallosilicate catalyst composite for alkylaromatic conversion, process for the preparation thereof, and use thereof in hydrocarbon conversion |
DE10132499A1 (de) * | 2001-07-05 | 2003-01-23 | Basf Ag | Verfahren zur selektiven Synthese von Triethylendiamin |
JP4170734B2 (ja) * | 2002-11-13 | 2008-10-22 | 信越化学工業株式会社 | 多孔質膜形成用組成物、多孔質膜とその製造方法、層間絶縁膜及び半導体装置 |
JP4170735B2 (ja) * | 2002-11-13 | 2008-10-22 | 信越化学工業株式会社 | ゼオライトゾルとその製造方法、多孔質膜形成用組成物、多孔質膜とその製造方法、層間絶縁膜及び半導体装置 |
DE10303696A1 (de) | 2003-01-30 | 2004-08-12 | Basf Ag | Entfärbung und Farbstabilisierung von TEDA-Lösung |
US7049260B2 (en) * | 2003-06-03 | 2006-05-23 | Chevron Phillips Chemical Company Lp | Selective para-xylene production via methylation of toluene with methanol in the presence of modified HZSM-5 catalyst |
DE10326137A1 (de) * | 2003-06-06 | 2004-12-23 | Basf Ag | Verfahren zur Erhöhung der Schneidhärte eines Formkörpers enthaltend ein kristallines Alumosilikat und Verwendung dieser Formkörper mit erhöhter Schneidhärte in chemischen Syntheseverfahren, insbesondere in einem Verfahren zur Herstellung von Triethylendiamin (TEDA) durch Umsetzung von Ethylendiamin (EDA) und/oder Piperazin (PIP) |
US7393978B2 (en) | 2003-08-01 | 2008-07-01 | Basf Aktiengesellschaft | Method for producing ethylene-amines |
DE10356184A1 (de) | 2003-12-02 | 2005-07-07 | Basf Ag | Zeolithisches Material vom Pentasil-Strukturtyp, seine Herstellung und seine Verwendung |
DE102004024274A1 (de) | 2004-05-15 | 2005-12-01 | Basf Ag | Verfahren zur Herstellung einer Lösung von reinem Triethylendiamin (TEDA) |
DE102004029544A1 (de) * | 2004-06-18 | 2006-01-05 | Basf Ag | Formkörper enthaltend ein mikroporöses Material und mindestens ein siliciumhaltiges Bindemittel, Verfahren zu seiner Herstellung und seine Verwendung als Katalysator, insbesondere in einem Verfahren zur Herstellung von Triethylendiamin (TEDA) |
CN100425342C (zh) * | 2005-04-21 | 2008-10-15 | 上海华谊丙烯酸有限公司 | 一种沸石催化剂在二氢吡喃衍生物水解反应中的应用 |
KR101098495B1 (ko) * | 2005-08-15 | 2011-12-26 | 상하이 리서치 인스티튜트 오브 페트로케미칼 테크놀로지 시노펙 | 톨루엔 형태 선택성 알킬화반응에 의한 파라-자일렌 제조용촉매의 제조방법 |
CN102600884A (zh) * | 2012-03-13 | 2012-07-25 | 河北科技大学 | 一种乙二胺合成哌嗪催化剂的制备方法 |
CN103240116B (zh) * | 2013-04-24 | 2015-04-29 | 北京化工大学 | 一种用于生产哌嗪和三乙烯二胺的催化剂及制备方法 |
CN106164042A (zh) * | 2014-04-03 | 2016-11-23 | 巴斯夫欧洲公司 | 通过胺混合物在沸石催化剂上反应而制备teda |
CN106831794B (zh) * | 2017-01-20 | 2019-03-05 | 万华化学集团股份有限公司 | 一种制备哌嗪和三乙烯二胺的方法 |
CN109422705B (zh) * | 2017-08-22 | 2022-11-08 | 中国科学院大连化学物理研究所 | 无溶剂条件下由乙二胺催化合成哌嗪和三乙烯二胺的方法 |
CN108465485B (zh) * | 2018-03-26 | 2021-10-22 | 泉州师范学院 | 用于乙醇胺环化合成三乙烯二胺的催化剂及其制备方法和应用 |
CN111099615B (zh) * | 2018-10-25 | 2021-11-30 | 中国石油化工股份有限公司 | 介孔y分子筛的制备方法 |
CN116060101A (zh) * | 2021-10-31 | 2023-05-05 | 中国石油化工股份有限公司 | 一种合成二苯胺的催化剂、其制备方法和应用 |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR511167A (fr) * | 1918-01-12 | 1920-12-18 | Commw Steel | Construction perfectionnée de wagon |
DE423526C (de) * | 1923-07-07 | 1926-01-05 | Georges Emile Massin | Drehbarer Scheinwerfer fuer Kraftfahrzeuge |
JPS5337876B2 (de) * | 1973-07-19 | 1978-10-12 | ||
JPS60260574A (ja) * | 1984-04-10 | 1985-12-23 | ユニオン・カ−バイド・コ−ポレ−シヨン | 1−アザビシクロ〔2.2.2〕オクタン又は1,4−ジアザビシクロ〔2.2.2〕オクタンの合成 |
US5041548A (en) * | 1985-12-05 | 1991-08-20 | Idemitsu Kosan Company Limited | Method for the preparation of triethylene diamines |
US4804758A (en) * | 1986-10-08 | 1989-02-14 | Basf Aktiengesellschaft | Preparation of 1,4-diazabicyclo[2.2.2]octanes |
JPH0633266B2 (ja) * | 1986-11-10 | 1994-05-02 | 出光興産株式会社 | トリエチレンジアミン類の製造方法 |
DE3735214A1 (de) * | 1987-10-17 | 1989-04-27 | Huels Chemische Werke Ag | Verfahren zur herstellung von 1,4-diazabicyclo(2.2.2)-octan aus piperazin |
DE3735212A1 (de) * | 1987-10-17 | 1989-04-27 | Huels Chemische Werke Ag | Verfahren zur herstellung von gemischen aus 1,4-diazabicyclo(2.2.2)-octan und piperazin |
US5382696A (en) * | 1992-10-16 | 1995-01-17 | Mitsui Toatsu Chemicals, Incorporated | Method for preparing methylamines |
US5365004A (en) * | 1993-05-28 | 1994-11-15 | Mobil Oil Corp. | Selective toluene disproportionation process (STDP) with ex situ selectivated zeolite catalysts |
US5567666A (en) * | 1995-05-15 | 1996-10-22 | Mobil Oil Corporation | Selectivated zeolite catalyst treated with a dealuminizing agent |
US5731449A (en) * | 1996-09-23 | 1998-03-24 | Air Products And Chemicals, Inc. | Triethylendiamine synthesis with base-treated zeolites as catalysts |
US5741906A (en) * | 1996-11-15 | 1998-04-21 | Air Products And Chemicals, Inc. | Production of triethylenediamine using surface acidity deactivated zeolite catalysts |
-
1998
- 1998-04-09 US US09/057,662 patent/US6084096A/en not_active Expired - Fee Related
-
1999
- 1999-04-07 KR KR1019990011944A patent/KR100322780B1/ko not_active IP Right Cessation
- 1999-04-08 JP JP10081399A patent/JP3883326B2/ja not_active Expired - Fee Related
- 1999-04-08 EP EP99106963A patent/EP0952152B1/de not_active Expired - Lifetime
- 1999-04-08 DE DE69905962T patent/DE69905962T2/de not_active Expired - Fee Related
- 1999-04-09 CN CN99104982A patent/CN1121400C/zh not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
CN1121400C (zh) | 2003-09-17 |
KR19990082983A (ko) | 1999-11-25 |
US6084096A (en) | 2000-07-04 |
DE69905962T2 (de) | 2003-09-11 |
EP0952152A3 (de) | 2000-02-23 |
JPH11349578A (ja) | 1999-12-21 |
JP3883326B2 (ja) | 2007-02-21 |
KR100322780B1 (ko) | 2002-03-18 |
EP0952152B1 (de) | 2003-03-19 |
CN1234401A (zh) | 1999-11-10 |
EP0952152A2 (de) | 1999-10-27 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
DE69905962T2 (de) | Synthese von Triethylendiamin und Piperazine mit Hilfe von mit Silicium enthaltende Verbindungen modifizierten Zeolith Katalysatoren | |
ATE255536T1 (de) | Synthetisches poröses kristallines mcm-68, synthese und verwendung desselben | |
DE69924930D1 (de) | Synthese von Oligonukleotiden | |
ATE233269T1 (de) | Regioselektive synthese von rapamycinderivaten | |
ATE337090T1 (de) | Synthese von molekularsiebkatalysatoren | |
DE69916582D1 (de) | Synthese von zsm-48 | |
DE60003874D1 (de) | Resistmaterialien und Verbindungen | |
DE69502726D1 (de) | Hestellung von aniontensidgranulaten | |
DE69507502D1 (de) | Synthese von porösen, kristallinen feststoffen in ammoniak | |
EE200300167A (et) | Amidoalküülpiperidiini ja -piperasiini derivaadid, neid sisaldav farmatseutiline kompositsioon ningühendite kasutamine närvisüsteemi häirete raviks | |
DE69019745T2 (de) | Synthese von carbonylverbindungen. | |
DE60236458D1 (de) | Pyrrolopyrimidin a2b selektive antagonistische verbindungen, deren synthese und verwendung | |
ATE242750T1 (de) | Synthese von kristallinen silicoaluminophosphaten | |
DE69223684T2 (de) | Synthese von Squaryliumverbindungen | |
DE69912206D1 (de) | Verbesserte Synthese von Haloformiminverbindungen | |
DE59702986D1 (de) | Synthese von aromatischen Aminen aus Chloraromaten | |
DE69713697T2 (de) | Synthese von Triethylendiamin mit Base behandelten Zeolithen | |
DE69808166D1 (de) | Katalysator und Wabenkörper-, Bettkatalysatoreinheit aus Metal hierfür | |
DE69602937T2 (de) | Verbesserte synthese von racemischen metallocenen | |
DE10084931T1 (de) | Fliessbettkatalysator für die Ammoxidation von Propylen zu Acrylonitril | |
DE3783084T2 (de) | Chirale phosphinopyrrolidin-verbindungen und ihre verwendung fuer asymetrische synthese optisch aktiver verbindungen. | |
DE60144573D1 (de) | Verfahren und Zwischenprodukte bei der Synthese von L-Thymidin | |
DE69706531D1 (de) | Bis alkenyl-derivate, flüssigkristalline verbindungen und flüssigkristalline zusammensetzungen | |
DE69722585D1 (de) | Synthese von wellenformen | |
DE69901444D1 (de) | Chemische synthese von morpholinderivaten |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition | ||
8339 | Ceased/non-payment of the annual fee |